LipidDoc_ATL said:Reconstituted peptide stability data for certificates of analysis: I had Janoshik test my reconstituted vial at day 1, day 14, and day 28 stored in…
Community-verified vendors for certificates of analysis: I maintain a spreadsheet of Janoshik-verified test results submitted by community members. Across 48 submitted tests:
- 85% tested at ≥98% purity
- 10% tested at 95-98% purity
- 5% tested at <95% purity (concerning)
The vendors with consistently high purity results are listed in the Vendor Directory. We update monthly based on new community submissions.
mike_nyc said:One addition: an unstated method makes a report close to uninterpretable.
This answered a question I did not know how to ask. Printing the relevant bit and taking it with me.
LipidDoc_ATL said:Reconstituted peptide stability data for certificates of analysis: I had Janoshik test my reconstituted vial at day 1, day 14, and day 28 stored in…
I tested my certificates of analysis batch through Janoshik — 99.8% purity. That's within acceptable range for compounded peptides. Turnaround was 14 business days.
The test costs ~$128 but gives you actual HPLC chromatography data plus mass spec confirmation. For the peace of mind alone, it's worth every penny. I test every new batch from a new vendor.
PeptideDetective — Independent Peptide Analytics
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View ResultsAttorneyGrant said:I have a certificate reporting 99.2% purity and 6.1mg content on a vial sold as 5mg, and I cannot work out whether those two numbers are consistent or…
COA red flags for certificates of analysis — here's what to look for when reviewing a Certificate of Analysis:
- No HPLC data: If there's no chromatography graph, it's not a real COA
- Exact 100% purity: Suspicious — real testing always shows slight variation
- No batch number: Can't trace back to specific production
- No endotoxin testing: For injectables, this is essential
- Template looks like it was made in Word: Professional labs have standardized formats
I have seen fake COAs that are literally photoshopped. Always verify independently if possible.